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Sep 2023;52(9):607-612

doi: 10.1016/j.metabol.2015.01.007 123 KohKKParkSMQuonMJ

The cell pellets were resuspended in 800 L of ice-cold 80% (v/v) methanol, mixed with 0.35 g of 0.2 mm zirconia-silica beads (BioSpec Products Inc., Bartlesville, OK, United States) in 1.5 mL microtubes, and cooled on ice